Fracture Toughness Of Specimens Research Articles

Experimental and numerical assessment of fracture toughness variations in steam boiler components after a long period of operation

This study presents an experimental and numerical assessment of the fracture toughness of steam boiler components, which have been in operation for more than 100,000 h. The materials tested are components of two different parts of a steam turbine unit: the pipeline section that connects the headers with turbines, which is made of 13HMF steel, and the valve chamber section, which is made of L17HMF steel grades. Full-size arc-shaped tension specimens (AT) are employed for the experimental evaluation. AT and single-edge notch tension (SENT) specimens are used for numerical assessment. The finite element method (FEM) formulations are developed and examined in Abaqus, which is set up as a shell model with the specimen thickness designated as the mid-surface for the analysis. The notch is modeled using a contour integral definition based on the maximum energy release rate criterion. The fracture toughness is quantified using the stress intensity factor (KI), and the results are compared. The valve chamber is found to have a higher fracture toughness than the pipeline section. The effect of specimen geometry is also noticeable, and the fracture toughness of SENT and AT specimens are compared. The results are useful in assessing the component’s durability after long operation.

Dynamic impact experimental and global cohesive element method to shale fracture characterization

The fracture behavior and various of mechanical mechanisms of shale are greatly influenced by the bedding surface. To study the effects of bedding angles on the crack propagation patterns and dynamic fracture properties, the shale notched semi-circular bend (NSCB) specimens were studied by the modified split Hopkinson pressure bar (SHPB) device, three-dimensional digital image correlation (3D-DIC) system with the high-speed (HS) photography and ABAQUS finite element software. The research results showed that at the same impact velocity, the 30°, 45° and 60° beddings played an obvious deflexion effect on the shale crack propagation. However, the 0° and 90° bedding did not deflect the crack propagation. The dynamic fracture toughness of shale NSCB specimens increased with the increase of impact loading rate but the increase magnitude decreased with the higher impact rate. The kinetic energy during specimen fracture was calculated by the extracting displacement data from the 3D-DIC, and it was found that the kinetic energy accounted for less than 6% of the absorbed energy during the dynamic compression of the shale. The crack propagation characteristics of ABAQUS simulation was approximately consistent with the experimental results. It is conducive to the study of shale gas fracturing and the formation of complex seam networks in shale and it is of great research significance for the efficient extraction of shale gas.

Dynamic fracture properties and criterion of cyclic freeze-thaw treated granite subjected to mixed-mode loading

Rock masses in high-elevation or cold regions are vulnerable to the combined effects of freeze-thaw (F-T) weathering and dynamic mixed-mode loading, posing a serious threaten to the safety and stability of geotechnical engineering. In this study, a series of dynamic fracture tests were conducted on notched semi-circular bend (NSCB) granite specimens subjected to different mixed-mode loading and F-T cycles using a split Hopkinson pressure bar (SHPB) test system. The effects of F-T treatment and dynamic mixed-mode loading on the fracture properties of granite, including effective fracture toughness, progressive fracture process, and macroscopic morphology of fracture surface, were comprehensively revealed. The experimental results suggest that the dynamic effective fracture toughness of NSCB specimens is dependent on the loading rate, particularly when the mode I loading is dominant. Additionally, the fracture toughness decreases as the number of F-T cycles increases, with an inflection point at 30 F-T cycles. All granite specimens subjected to mixed-mode loading exhibit a curved fracture path, with faster crack propagation speed and more fine cracks in specimens exposed to higher F-T cycles. Macroscopic morphology of fracture surface obtained using three-dimensional (3D) scanning indicates that the fractal dimension of the fracture surface increases with increasing F-T cycles, and the increment is more pronounced for specimens subjected to a higher mode II loading component. Moreover, this study compared the fracture resistance of F-T treated granite subjected to dynamic mixed loading using the maximum tangential stress (MTS) criterion and the generalized maximum tangential stress-based semi-analytical (SA-GMTS) criterion. Compared with the MTS criterion, the SA-GMTS criterion shows a more reasonable consistency with the experimental results, with a root mean square error within ±7%.

A study of microstructure and mechanical properties of (CoCrNi)82Al9Ti9 high entropy alloy by electrical-thermal-mechanical coupled rapid post-treatment

In this work, we have creatively used electrical-thermal-mechanical coupled rapid post-treatment to improve the properties of (CoCrNi)82Al9Ti9 high entropy alloy (HEA). The effect of the electrical-thermal-mechanical coupled field on the phase, microstructure, microhardness, fracture toughness, and compression properties of SLM specimens are investigated. The results show that the SLM specimen exhibits face-centered cubic (FCC) and body-centered cubic (BCC) phases and the microstructure is a dendrite structure. The SLM specimens exhibit imperfections, including porosity and cracks, as well as low densification. After electrical-thermal-mechanical coupled rapid post-treatment, the FCC phase decreases while the BCC phase increases in the SLM specimen, and the microstructure changes from dendritic to recrystallized. The created specimens are healed of defects and the densification is increased to 99.6%. It can be attributed to the combination of the electrical (Electron wind) and thermal effects (Joule heat) of pulse current. Electron wind promotes the diffusion of atoms and expansion of the movement of dislocations, providing the material basis for defect healing and recrystallization. Joule heat provides the substance conditions. The (CoCrNi)82Al9Ti9 HEA has a remarkable improvement in strength and ductility.

Investigation on interlayer debonding behavior of unidirectional composite laminates under cyclical hygrothermal aging duration effects

AbstractThe composite interlamination is the key part of load transfer and plays a decisive role in the overall mechanical performance of composite structures. The interlaminar property is predominantly influenced by the matrix resin which is easily affected by the hygrothermal environment. This paper delved into the effect of hygrothermal aging duration on the interlayer debonding behavior of unidirectional (UD) laminates. The pre‐cracked specimens were treated by hygrothermal aging with a period of 0, 15, 30, 60, 90, and 120 days. The double cantilever beam (DCB) tests were employed to evaluate the interlaminar property. The effect of hygrothermal aging on load–displacement responses, R‐curves, crack growth speed, and fracture surface topography was analyzed. The results revealed that the load‐bearing capacity of aged specimens presented a reduction of 18.6%–29.0% compared with unaged ones. The interlaminar fracture toughness of specimens subjected to 15 days of treatment decreased significantly compared with that of unaged specimens due to the increase of water absorption caused by hygrothermal aging. With the increase in hygrothermal aging time, the interlaminar fracture toughness peaked at 60 days because of the post‐curing effect, followed by a declining trend influenced by the dominant hygrothermal aging effect. The fiber bridging of aged samples was increasingly obvious, became the most prominent at 60 days, and then gradually reduced. The fiber bridging diminished the crack propagation speed, hindered interlaminar debonding, and contributed to the interlaminar toughening.Highlights The samples underwent hygrothermal aging for 0, 15, 30, 60, 90, and 120 days. Load ability of aged samples was at least 18.6% lower than that of unaged ones. R‐curves rose before the crack length of 79 mm and then tended to stabilize. Fracture toughness first decreased, then increased and reduced with aging time. Fiber bridging could hinder crack growth and improve the interlayer property.

An experimental evaluation on rate sensitivity of fracture toughness in sheet specimens made of SUS304 metastable austenitic stainless steel

Utilizing transformation-induced plasticity (TRIP) steel with strain-induced martensitic transformation (SIMT) on automotive steel plates and developing products which have exceptional energy absorption capabilities can be used to reduce weight. For this purpose, it is important to clarify the fracture toughness of TRIP steels and its strain rate dependency to ensure the use of impact-absorbing members over a wide range of deformation rates. However, inconsistent rate dependent trends were observed in the previous studies, possibly as a result of the transition of the fracture mode. Therefore, the effect of fracture modes and strain rate on the fracture toughness values needs to be examined sufficiently. In the present study, the fracture toughness of the specimens made of SUS304 metastable austenitic stainless steel, which is a kind of TRIP steel, is evaluated by tensile tests at various strain rates. Direct current potential difference and digital image correlation methods are introduced to detect the time of fracture initiation during deformation, especially at high deformation rates by using the developed impact tensile tests based on the split Hopkinson pressure bar. The fracture surfaces of the fractured specimens are observed by using an electron scanning electron microscopy to determine not only the fracture modes and their rate dependent effects but also the reinforcement mechanism of SIMT in mixed modes. The results demonstrate that fracture toughness shows negative strain rate dependency, and mixed-mode fracture can be found near the crack in the case of the impact tensile test.

A phase-field fatigue fracture model considering the thickness effect

Modern aero-engine turbine structures often have variable-thickness geometries (e.g., turbine structures with complex cooling systems) that pose a significant challenge to crack analysis. The phase-field fracture method is a numerical method that has recently received considerable attention. However, phase-field fatigue fracture models that consider the effect of thickness are still lacking. To address this problem, this paper proposes a modification of the fracture toughness in the phase-field fatigue model by introducing a relationship function between material fracture toughness and thickness (Gc-B curve). We use reference experimental data to fit the Gc-B curve of GH4169 and predict the fracture toughness of specimens with other thicknesses. The predictions of the proposed model agree well with the experimental results reported in the literature. This achievement contributes significantly to the structural safety design and life prediction of aero-engine components.

Experimental evaluation of fracture toughness of basalt macro fiber reinforced high performance lightweight aggregate concrete

High performance lightweight aggregate concrete has become a popular topic for the development of green concrete due to the incorporation of various industrial wastes to substitute aggregate. However, its brittleness has gradually emerged as an issue with the increasing of compressive strength. To address this concern, the authors in this paper investigated the influence of basalt macro fiber (BMF) on the compressive and splitting tensile strengths of lightweight aggregate concrete at different fiber volume contents and lengths. Moreover, the three-point bending test on notched beams, with the help of acoustic emission and digital image correlation, was also carried out to evaluate the fracture toughness of basalt macro fiber reinforced lightweight aggregate concrete. Finally, the softening constitutive model was determined in the present study. The results showed that the addition of BMF increased the compressive strength of lightweight aggregate concrete and the maximum increase reached 9.03%. As for splitting tensile strength, the maximum increase was 39.88%. In addition, it was observed that the incorporation of basalt macro fiber significantly improved the initial cracking toughness and unstable fracture toughness of plain specimen. The fracture energy of BMF reinforced lightweight aggregate concrete was also increased, and the largest improvement was seen in BMF-0.5–22.5 group, 8.5 times that of plain specimen.

Degradation of SMA-13 low-temperature performance under coupled dry and wet-salt corrosion

To investigate the low-temperature performance of polyester fiber-modified asphalt mixtures under the influence of dry-wet-salt corrosion coupling, six different polyester fiber content levels (0%, 0.3%, 0.35%, 0.4%, 0.45%, and 0.5% by weight of the mixture) were chosen for preparing SMA-13 asphalt mixture specimens. The Ultrasonic non-destructive testing, semi-circular bending tests, and scanning electron microscopy (SEM) were employed to evaluate the low-temperature performance of these mixtures under dry-wet-salt corrosion conditions with varying cycle numbers (0, 2, 4, 6, 8 cycles). The results of ultrasonic non-destructive testing showed that the wave velocity exhibited a trend of initial increase followed by a subsequent decrease with the increase in polyester fiber content. It reached a maximum value of 4.06 cm/us at a fiber content of 0.4%. The semi-circular bending tests (SCB) revealed that the fracture toughness of the polyester fiber asphalt mixture decreased as the number of dry-wet cycles increased. The impact of salt-dry-wet coupling > water-dry-wet coupling. Notably, after undergoing 4 cycles of water-dry-wet exposure, the overall fluctuation in specimen fracture toughness was minimal, indicating that results after four cycles could be suitable for evaluating the long-term degradation performance of asphalt mixtures under extended water-dry-wet cycling. SEM test results demonstrated that a polyester fiber content of 0.4% led to the formation of a strong fibrous network structure within the asphalt mixture. This significantly reduced moisture and salt intrusion during the dry-wet cycling process, enhancing the low-temperature crack resistance of the specimens.

Hygrothermal effects on translaminar fracture toughness of quasi-isotropic laminates with different stacking sequences

Hygrothermal effects on the translaminar fracture toughness of the carbon/epoxy composite with two different stacking sequences at 120 °C were studied and the failure mechanisms are explained. The eccentrically loaded single-edge-notch tension (ESET) experiments showed that two different quasi-isotropic stacking sequences ([90/45/0/-45]4s and [45/90/-45/0]4s) have negligible difference in translaminar fracture toughness. It was found that the fracture toughness of conditioned specimens at hot temperature wet (HTW) condition increased by 75 % compared to that at room temperature dry (RTD). The average saturated damage height at HTW increased by 48 % compared with that at RTD according to ex situ X-ray computed tomography (CT) observation. The larger saturated damage height observed in the 0° plies of the HTW specimens results in the higher translaminar fracture toughness.

Effect of final temperature and heating rate on the mechanical and optical properties of a zirconia veneering ceramic

PurposeTo evaluate the effect of firing temperature and heating rate on the volumetric shrinkage, translucency, flexural strength, hardness, and fracture toughness of a zirconia veneering ceramic. Material and methodsZirconia veneering ceramic specimens (N = 45) with varying final temperatures (730 °C, 750 °C, and 770 °C) and heating rates (70 °C/min, 55 °C/min, and 40 °C/min) were fabricated (n = 5). Each specimen's shrinkage, translucency, flexural strength, hardness, and fracture toughness were determined. Two-way analysis of variance, Scheffé test, and Pearson's correlation analysis were used to evaluate data (α = 0.05). ResultsThe shrinkage (44.9 ± 3.1–47.5 ± 1.6 vol%) and flexural strength (74.1 ± 17.4–107.0 ± 27.1 MPa) were not affected by tested parameters (P ≥ 0.288). The interaction between the main factors affected the translucency, hardness, and fracture toughness of the specimens (P ≤ 0.007). Specimens with 770 °C final temperature and 70 °C/min heating rate had the lowest (21.8 ± 3.2 %) translucency (P ≤ 0.039). The hardness ranged between 4.98 ± 0.51 GPa (730 °C; 70 °C/min) and 5.60 ± 0.37 GPa (770 °C; 70 °C/min). Fracture toughness ranged between 0.54 ± 0.04 MPa√m and 0.67 ± 0.08 MPa√m with the highest values for specimens fired at 730 °C with 70 °C/min (P ≤ 0.001). There was a positive correlation between translucency and hardness (r = 0.335, P = 0.012), and a negative correlation between fracture toughness and all parameters other than shrinkage (translucency: r = −0.693/P < 0.001, flexural strength: r = −0.258/P = 0.046, hardness: r = −0.457/P < 0.001). ConclusionsHeating rate and final temperature should be considered while fabricating veneered zirconia restorations with tested ceramic as they affected the translucency, hardness, and fracture toughness.

Edge notched disc test for evaluation of mode-I fracture toughness of brittle material

In the current investigation, the fracture toughness of plexiglass specimens was accurately measured employing Edge Notched Disc (END) type specimens. Besides, the Notched Brazilian Discs (NBD) were used in order to validate the results of the conducted END experiments. Moreover, a numerical analysis was carried out on the END tests to verify the accuracy of the measured fracture toughness values. In the first stage, the splitting tensile test was used to accurately calibrate the micro-scale properties of the Flat Joint (FJ) model. In the second phase, the numerical simulation of END and NBD models was created, in which the notch lengths in END and NBD were set to 5, 15, 25, 40 and 10, 20, 30, 40, 50, 60 in millimeters, respectively. According to the obtained results, the considered FJ model is capable of making an accurate determination of the potential crack growth path and crack initiation stress like the experimentally obtained results for plexiglass specimens. It was also derived that lengthening the notch could not have a considerable effect on the fracture toughness of the models. The Tensile stress distribution on the failure surface of END test could be the main cause of the lower fracture toughness levels of END test. Besides, the same fracture extension patterns were seen from the experimental investigations and numerical simulations.

Constraint loss correction: Enhancing transferability of fracture toughness of Eurofer97 compact tension specimens between specimen sizes

This paper proposes and implements a constraint loss correction as a supplement to the ASTM correction factor for the master curve method (ASTM-E1921) for Eurofer97 reduced activation steel in order to enhance the transferability of results between compact tension (CT) specimen sizes. To facilitate the acquisition and scalability of reliable fracture toughness data from one specimen size to another and to apply the Master-Curve method with confidence when using small specimens, the difference in the structure of the crack tip stress field between large and small specimens was modeled. The stress intensity factors and critical volumes/stresses of two specimen sizes (1 T and 0.18 T) were calculated with 3D finite element simulations run over a large displacement range and at a temperature range of −120 to −80 °C and the results were compared with real data from a database of toughness tests of Eurofer97 steel. The K values from a miniaturized specimen without or with ASTM correction and with the proposed combined correction with constraint loss factor (which is variable over the entire loading range) were compared with simulated CT-1 T stress intensity values. It was found that this new correction factor was accurate up to a target toughness of 200 MPa.m1/2, which represents a major improvement on the current state of the art.

Effect of aging on the low-temperature performance of fiber-reinforced asphalt mixtures

To study the effect of aging on the low-temperature crack resistance of fiber asphalt mixes, three kinds of fibers (lignin fiber, polyester fiber, and basalt fiber) were dry blended into AC-13 asphalt mixes to prepare unaged, asphalt aged (that is, the original asphalt material is subjected to aging treatment), short-term aged, and long-term aged fiber reinforced asphalt mixes. Semicircular bending (SCB) tests and scanning electron microscopy tests were used to analyze and study the effects of aging time and fiber type on the low-temperature properties of asphalt mixtures at an ambient temperature of −5 °C. The SCB test results indicated that: with the deepening of aging, the fracture toughness and fracture energy of the fiber asphalt mixture specimens will tend to decrease, and the aging of the original asphalt has a greater impact on the specimens without fiber; there was great variability in the effect of lignin fibers on the crack resistance of the mix, but it could be a good promoter in unaged asphalt mixes; polyester fiber is the material of choice for improving low-temperature crack resistance in long-term aging pavements; the incorporation of basalt fiber greatly enhances the crack resistance of asphalt mixes and is an excellent material for improving aging asphalt mixes. It is clearly seen by the scanning electron microscope test that with the deepening of aging, the adhesion of asphalt and aggregate gradually deteriorates, and even more so, there is the phenomenon of fine aggregate flaking, and the fiber cannot play an excellent role in reinforcement and crack resistance.

Numerical investigation on spall fracture in metallic materials due to laser shock peening via phase field approach to fracture

Laser shock peening (LSP) is an effective surface reinforcement technique for metallic materials. However, when LSP is applied to a thin specimen, an undesirable result, spall fracture, may occur. In this work, the spall fracture generated in multiple-shock LSP processes is investigated via the phase field approach to fracture, and is validated with the experimental result. In particular, the relations between the formation of spall fracture and the shock number, the shock wave pressure, the specimen thickness and the fracture toughness of specimen are studied. The results indicate that the formation of spall fracture in multiple-shock processes is an accumulative process, and is mainly influenced by the shock wave pressure and the specimen thickness, and multiple shocks will complicate the interaction between the tensile wave tail and the compressive wave front of the shock wave, leading to an enlargement of the spall fracture region.

A new technique to measure the dynamic fracture toughness of solids

We propose and assess a new experimental technique to measure the fracture toughness of engineering materials and its sensitivity to strain rate. The proposed method is based on a ring expansion technique and it overcomes the limitations of current dynamic fracture tests, as it is not affected by transient stress wave propagation during loading and it results in spatially uniform remote stress and strain fields prior to fracture; the method is also suitable to achieve remote strain rates well in excess of 1000 s−1. We demonstrate the technique by measuring the plane-stress Mode I fracture toughness of PMMA specimens at remote strain rates ranging from 10−3 s−1 to 102 s−1. The experiments show an increase of the toughness of the material with increasing strain rate.

Study on the effects of microstructures on the fracture behavior of an Al-Cu-Mg alloy

In this study, a special fracture delamination in L-T fracture toughness specimens of an Al-Cu-Mg alloy was researched by applying three-dimensional optical microscopy (OM), scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD) methods. The results indicate that the fracture delamination is contributed by the cracks extending a long distance in the T-direction and extending internally along the L-direction, which can result in a lower fracture toughness value. The fracture delamination is determined by the level of grain flattening and the distribution of the second phases. The flat grains result in a tendency for cracks to extend in the T-direction. At the same time, the unevenly distributed Al2Cu and Al2CuMg phases lead to cracks extending in the L-direction, which eventually causes the formation of delamination fractures. The reduction in grain size can also contribute to weakening the fracture delamination to a certain extent.

An integrated experimental-computational framework to assess the influence of microstructure and material properties on fracture toughness in clinical specimens of human femoral cortical bone

Microstructural and compositional changes that occur due to aging, pathological conditions, or pharmacological treatments alter cortical bone fracture resistance. However, the relative importance of these changes to the fracture resistance of cortical bone has not been quantified in detail. In this technical note, we developed an integrated experimental-computational framework utilizing human femoral cortical bone biopsies to advance the understanding of how fracture resistance of cortical bone is modulated due to modifications in its microstructure and material properties. Four human biopsy samples from individuals with varying fragility fracture history and osteoporosis treatment status were converted to finite element models incorporating specimen-specific material properties and were analyzed using fracture mechanics-based modeling. The results showed that cement line density and osteonal volume had a significant effect on crack volume. The removal of cement lines substantially increased the crack volume in the osteons and interstitial bone, representing straight crack growth, compared to models with cement lines due to the lack of crack deflection in the models without cement lines. Crack volume in the osteons and interstitial bone increased when mean elastic modulus and ultimate strength increased and mean fracture toughness decreased. Crack volume in the osteons and interstitial bone was reduced when material property heterogeneity was incorporated in the models. Although both the microstructure and the heterogeneity of the material properties of the cortical bone independently increased the fracture toughness, the relative contribution of the microstructure was more significant. The integrated experimental-computational framework developed here can identify the most critical microscale features of cortical bone modulated by pathological processes or pharmacological treatments that drive changes in fracture resistance and improve our understanding of the relative influence of microstructure and material properties on fracture resistance of cortical bone.

Pressure reduction strategy based on a new CTOD model considering room temperature creep for X80 pipeline steel

The growing demand for energy consumption has led to the rapid development of high strength and high toughness pipeline steel technology, with fracture toughness being a crucial factor in evaluating the mechanical properties of pipeline steel. Despite experimental studies demonstrating that metallic materials, including pipeline steel, undergo creep at room temperature, the effects of room temperature creep (RTC) on pipeline steel fracture properties are still relatively unexplained. This study analyzes the impact of RTC on the fracture toughness of X80pipeline steel, using the X80pipeline steel base material as the research object. Firstly, the time-dependent change in crack notch opening displacement is added to the calculation formula for fracture toughness of three-point bending specimens, considering the effect of RTC. The test data is fitted to a power-law equation of the form, where k=0.01423 and m=-0.89651, with the improved formula indicating an incremental CTOD of approximately 0.0098 mm after 36 h of RTC for X80 pipeline steel. Secondly, a time-dependent CTOD model is proposed based on the ductile defect growth model, with the plastic part derived from the D-B model and the creep part obtained by fitting the test data. The study proposes a CTOD criterion for RTC and a pressure reduction strategy based on this criterion, providing a reference for quantitatively assessing the fracture toughness of pipeline steel under RTC conditions.

Influence of hybrid nano/micro particles on the mechanical performance of cross-ply carbon fibre fabric reinforced epoxy polymer composite materials

This study presents the flexural strength, compressive strength, and impact energy behaviour of graphene nanoplates and fly ash microparticle-loaded cement-based CFRP composites manufactured by the vacuum-assisted resin infusion method (VARIM). The composite structures consist of a fixed ratio of graphene nanoplates (2%), fly ash (2%), silica (2%), cement (2%), and sand (4%) particles filled into cross-plied carbon fibre-reinforced epoxy resin polymer composite beams and columns. Composites fabricated by hand lay-up methods because of infiltration problems. A three-point bending test through the width was used to measure the flexural strength of the graphene nanoplate (GnP)-filled CFRP composite beam. The low-velocity Izod impact and Charpy impact tests through the thickness were used to determine Charpy impact energy (3.46 J), Izod impact energy (2.5 J), and the dynamic fracture toughness of notch specimens under Charpy (28.5 KJ/m2) and Izod impact (25.0 KJ/m2). Also, the compressive test method was used to measure the compressive strength of hybrid particles and short glass fibre-reinforced epoxy resin composite square and circular columns. The results show compressive strength and flexural strength. Izod impact energy, Charpy impact energy, and dynamic fracture toughness of hybrid nano/microparticle-filled fibre composites have higher values than virgin fibre composites because of the influence of graphene nanoparticles and the perfect interface bonding between two dissimilar molecules of nano and microparticles, which improve the fracture toughness and absorb impact energy. Overall, the results show that molecules of nano/microparticle-filled carbon fibre and glass fibre-reinforced epoxy resin composites can be used in seismic wave resistance because of their improved mechanical properties compared to virgin fibre composites. In addition, SEM micrographs clearly show that nano- and microparticles are resistant to crack propagation and the debonding of matrix fibres.